Method Development Validation Gas by Mishra Garima (12 results)
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Published by LAP LAMBERT Academic Publishing 2013-11-27, 2013
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Published by VDM Verlag Dr. Mueller Aktiengesellschaft & Co. KG, 2013
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Published by LAP LAMBERT Academic Publishing Nov 2013, 2013
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Taschenbuch. Condition: Neu. This item is printed on demand - it takes 3-4 days longer - Neuware -Residual solvents in pharmaceutical samples are monitored using gas chromatography with head space. Based on good manufacturing practices, measuring residual solvents is mandatory for the release testing of all active pharmaceutical… ingredients (API). The analysis of residual organic solvents (methanol, ethanol, acetone and toluene) in Omeprazole API was investigated.The Head space gas chromatography (HSGC) method described in this investigation utilized a DB - 624, 30 m long x 0.32 mm internal diameter, 1.8 mim thick column. Since Omeprazole is a thermally labile compound, the selection of the proper injector temperature is critical to the success of the analysis. The injector temperature was set at 180°C to prevent degradation. The initial oven temperature was set at 50°C for 10 min and programmed at a rate of 30°C min-1 to a final temperature of 200°C for 10 min. Nitrogen was used as a carrier gas and flame ionization detector was used. N,N-dimethyl formamide was selected as a diluent. The method was validated according to ICH guidelines and found to be specific, linear i.e.,C.C is 0.998,% RSD of each analyte is less than 8%, sensitive, rugged and showed excellent recovery. 96 pp. Englisch.
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Condition: New. Dieser Artikel ist ein Print on Demand Artikel und wird nach Ihrer Bestellung fuer Sie gedruckt. Autor/Autorin: Mishra GarimaThe author is Garima Mishra D/o Kashi Prasad Mishra, has completed her B.Pharm (2006-2010) from Lloyd institute of management and technology, Gr. Noida with 75.3%. She has completed M.Pharm…a (Pharmaceutical Chemistry) fr.
Language: English
Published by VDM Verlag Dr. Mueller Aktiengesellschaft & Co. KG, 2013
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Condition: New. Print on Demand pp. 96 2:B&W 6 x 9 in or 229 x 152 mm Perfect Bound on Creme w/Gloss Lam.
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Published by VDM Verlag Dr. Mueller Aktiengesellschaft & Co. KG, 2013
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Condition: New. PRINT ON DEMAND pp. 96.
Language: English
Published by LAP LAMBERT Academic Publishing Nov 2013, 2013
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Taschenbuch. Condition: Neu. This item is printed on demand - Print on Demand Titel. Neuware -Residual solvents in pharmaceutical samples are monitored using gas chromatography with head space. Based on good manufacturing practices, measuring residual solvents is mandatory for the release testing of all active pharmaceutical ing…redients (API). The analysis of residual organic solvents (methanol, ethanol, acetone and toluene) in Omeprazole API was investigated.The Head space gas chromatography (HSGC) method described in this investigation utilized a DB - 624, 30 m long x 0.32 mm internal diameter, 1.8 ¿m thick column. Since Omeprazole is a thermally labile compound, the selection of the proper injector temperature is critical to the success of the analysis. The injector temperature was set at 180°C to prevent degradation. The initial oven temperature was set at 50°C for 10 min and programmed at a rate of 30°C min¿1 to a final temperature of 200°C for 10 min. Nitrogen was used as a carrier gas and flame ionization detector was used. N,N-dimethyl formamide was selected as a diluent. The method was validated according to ICH guidelines and found to be specific, linear i.e.,C.C is 0.998,% RSD of each analyte is less than 8%, sensitive, rugged and showed excellent recovery.VDM Verlag, Dudweiler Landstraße 99, 66123 Saarbrücken 96 pp. Englisch.
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Taschenbuch. Condition: Neu. Method development and validation by Gas chromatography-HeadSpace | Garima Mishra (u. a.) | Taschenbuch | 96 S. | Englisch | 2013 | LAP LAMBERT Academic Publishing | EAN 9783659492914 | Verantwortliche Person für die EU: preigu GmbH & Co. KG, Lengericher Landstr. 19, 49078 Osnabrück, mail[at]preigu[d…ot]de | Anbieter: preigu Print on Demand.
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Seller: AHA-BUCH GmbH, Einbeck, GermanyAHA-BUCH GmbH
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Taschenbuch. Condition: Neu. nach der Bestellung gedruckt Neuware - Printed after ordering - Residual solvents in pharmaceutical samples are monitored using gas chromatography with head space. Based on good manufacturing practices, measuring residual solvents is mandatory for the release testing of all active pharmaceutical ingr…edients (API). The analysis of residual organic solvents (methanol, ethanol, acetone and toluene) in Omeprazole API was investigated.The Head space gas chromatography (HSGC) method described in this investigation utilized a DB - 624, 30 m long x 0.32 mm internal diameter, 1.8 mim thick column. Since Omeprazole is a thermally labile compound, the selection of the proper injector temperature is critical to the success of the analysis. The injector temperature was set at 180°C to prevent degradation. The initial oven temperature was set at 50°C for 10 min and programmed at a rate of 30°C min-1 to a final temperature of 200°C for 10 min. Nitrogen was used as a carrier gas and flame ionization detector was used. N,N-dimethyl formamide was selected as a diluent. The method was validated according to ICH guidelines and found to be specific, linear i.e.,C.C is 0.998,% RSD of each analyte is less than 8%, sensitive, rugged and showed excellent recovery.
