Synthesis and Characterization of Ultrafine TATB

Language: English

Published by LAP LAMBERT Academic Publishing Jun 2019, 2019

6202018704 / 9786202018708

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Seller: BuchWeltWeit Ludwig Meier e.K., Bergisch Gladbach, GermanyBuchWeltWeit Ludwig Meier e.K.

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Softcover

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This item is printed on demand - it takes 3-4 days longer - Neuware -An acid recrystallization process for synthesis of ultrafine TATB (UF-TATB) of median particle size 50 lm. PG-TATB is made soluble in DMSO-alkali. Acidification of this basic solution is done with dilute aqueous nitric acid, which causes precipitation of UF-TATB through a reaction crystallization process. The process is simple, economical, and easy to scale up. The effect of various process parameters such as acid concentration and neutralization time on particle size is studied and discussed. UF-TATB is characterized for purity, chloride content, particle size, DSC, STA, SEM, sensitivity, etc., and results have been compared with PG-TATB. Along with particle size, the chloride impurity in UF-TATB is also reduced from 0.7 to 0.13%. SEM analysis reveals regular bi-pyramidal shape with sharp edges and corners of UF-TATB crystals compared to porous and rough surfaces of PG-TATB crystals. There is an impact sensitivity gain in UF-TATB. This may be due to the ultrafine nature of the particles. 96 pp. Englisch.…

Seller Inventory # 9786202018708

Title
Synthesis and Characterization of Ultrafine TATB
Author
Amiya Nandi
Publisher
LAP LAMBERT Academic Publishing Jun 2019
Publication year
2019
Condition
Neu
Binding
Taschenbuch
Language
English
ISBN 10
6202018704
ISBN 13
9786202018708
Item weight
161 grams
Dimensions
220x150x7 mm

BuchWeltWeit Ludwig Meier e.K.

Bergisch Gladbach, Germany

5-star seller

AbeBooks seller since January 11, 2012

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BuchWeltWeit Ludwig Meier e.K.

Germany