As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.

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Title: Nuclear Magnetic Resonance
Publisher: Royal Society of Chemistry, GB
Publication Date: 1998
Language: English
ISBN 10: 0854043179
ISBN 13: 9780854043170
Binding: Hardback
Condition: New
Weight: 1912 grams

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For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage.

Excerpt. � Reprinted by permission. All rights reserved.

Nuclear Magnetic Resonance Volume 27

A Review of the Literature Published between June 1996 and May 1997

By G. A. Webb

The Royal Society of Chemistry

CHAPTER 1 NMR Books and Reviews By W. Schiff, 1, 
CHAPTER 2 Theoretical and Physical Aspects of Nuclear Shielding By C.J. Jameson, 44, 
CHAPTER 3 Applications of Nuclear Shielding By M. Yamaguchi, 83, 
CHAPTER 4 Theoretical Aspects of Spin-Spin Couplings By H. Fukui, 125, 
CHAPTER 5 Applications of Spin-Spin Couplings By K. Kamienska-Trela and J. Wojcik, 143, 
CHAPTER 6 Nuclear Spin Relaxation in Liquids and Gases By R. Ludwig, 199, 
CHAPTER 7 Solid State NMR By M.E. Smith, 222, 
CHAPTER 8 Multiple Pulse NMR By L.Y. Lian, 273, 
CHAPTER 9 NMR of Natural Macromolecules By P.C. Driscoll and S. M. Kristensen, 292, 
CHAPTER 10 Synthetic Macromolecules By H. Kurosu and T. Yamanobe, 337, 
CHAPTER 11 Conformational Analysis By J. R. P. Arnold and J. Fisher, 370, 
CHAPTER 12 Nuclear Magnetic Resonance Spectroscopy of Living Systems By M. J. W. Prior, 386, 
CHAPTER 13 Nuclear Magnetic Resonance Imaging By T. Watanabe, 431, 
CHAPTER 14 NMR of Paramagnetic Species By C. L. Khetrapal and K. V. Ramanathan, 458, 
Author Index, 485,

CHAPTER 1

NMR Books and Reviews

COMPILED BY W. SCHILF

1 Books

R1 F. A. Bovey and P. A. Mirau, 'NMR of Polymers', Academic, San Diego, Calif., 1996, 459 pp

2 Regular Review Series

Accounts of Chemical Research, 1996, vol. 29

R2 J. F. Haw, J. B. Nicholas, T. Xu, L. W. Beck and D. B. Ferguson, 'Physical Organic Chemistry of Solid Acids: Lessons From in Situ NMR and Theoretical Chemistry', p. 259

R3 A. G. Marshall, Ion Cyclotron Resonance and Nuclear Magnetic Resonance Spectroscopies: Magnetic Partners for Elucidation of Molecular Structure and Reactivity, p. 307

R4 J. Stubbe, J. W. Kozarich, W. Wu and D. E. Vanderwall, 'Bleomycins: A Structural Model for Specificity, Binding, and Double Strand Cleavage', p. 322

ACS Monographs, 1996, vol. 187

R5 T. S. Everett, 'Nuclear Magnetic Resonance Spectroscopy of Organofluorine Compounds', p. I 037

Advances in Chemistry Series, 1996, vol. 251

R6 H. A. Nasr-El-Din, 'Flow of Suspension in Pipelines', p. 177

Advances in Magnetic and Optical Resonance, ed. W. S. Warren, 1996, vol. 19

R7 F. Prigl and U. Haeberlen, 'The Theoretical and Practical Limits of Resolution in Multiple-Pulse High-Resolution NMR of Solids', p. 1

R8 S. J. Glaser and J. J. Quant, 'Homonuclear and Heteronuclear Hartmann-Hahn Transfer in Isotropic Liquids', p. 59

R9 P. T. Callaghan and J. Stepisnik, 'Generalized Analysis of Motion Using Magnetic Field Gradients', p. 325

Advances in Spectroscopy, 1996, vol. 25

R10 C. M. Spickett, W. E. Smith and J. Reglinski, 'Proton NMR Studies of Oxidative Stress in Disease', p. 267

R11 M. Grootveld, A. Sheerin, M. Atherton, A. D. Millar, E. J. Lynch, D. R. Blake and D. P. Naughton, 'Applications of High Resolution NMR Analysis to the Study of Inflammatory Diseases at the Molecular Level', p. 295

Annual Reports on Medicinal Chemistry, 1996, vol. 3I

R12 S. J. Archer, P. J. Domaille and E. D. Laue, 'New NMR Methods for Structural Studies of Proteins to Aid in Drug Design', p. 299

Annual Reports on NMR Spectroscopy, ed. G. A. Webb, 1996, vol. 32

R13 A. M. Gil, P. S. Belton and B. P. Hills, 'Application of NMR to Food Science', p. 1

R14 W. S. Price, 'Gradient NMR', p. 51

R15 D. J. Craik, K. J. Nielsen and K. A. Higgins, 'Pharmaceutical Applications of NMR', p. 143

R16 C. J. Groombridge, 'NMR Spectroscopy in Forensic Science', p. 215

Annual Reviews of Biophysics and Biomolecular Structure, 1996, vol. 25

R17 R. G. Bryant, 'The Dynamics of Water-Protein Interactions', p. 29

R18 A. Graeslund and M. Sahlin, 'Electron Paramagnetic Resonance and Nuclear Magnetic Resonance Studies of Class I Ribonucleotide Reductase', p. 259

Annual Reviews of Physical Chemistry, 1996, vol. 47

R19 C. J. Jameson, 'Understanding NMR Chemical Shifts', p. 135

R20 K. T. Dayie, G. Wagner and J-F. Lefevre, 'Theory and Practice of Nuclear Spin Relaxation in Proteins', p. 243

R21 H. J. Dyson and P. E. Wright, 'Insights into Protein Folding from NMR', p. 369

Comprehensive Supramolecular Chemistry, ed. G. Alberti and T. Bein, Elsevier, Oxford, UK, 1996, vol. 7

R22 D. N. Theodorou, R. Q. Snurr and A. T. Bell, 'Molecular Dynamics and Diffusion in Microporous Materials', p. 507

Comprehensive Supramolecular Chemistry, ed. J. Davies, D. Eric and J. A. Ripmeester, Elsevier, Oxford, UK, 1996, vol. 8

R23 E. A. C. Lucken, F. Grandjean and G. J. Long, 'NQR and Moessbauer Spectroscopy [In Supramolecular Chemistry]', p. 225

R24 D. D. Klug and J. S. Tse, 'High-Pressure Methods [In Supramolecular Chemistry]', p. 307

Coordination Chemistry Reviews, 1996, vol. 148

R25 A. Mori, K. Kubo and H. Takeshita, 'Synthesis and Metallophilic Properties of Troponoid Thiocrown Ethers', p. 71

R26 Y. Habata and S. Akabori, 'Alkylphosphoric Acid Armed Crown Ethers Having a Specific Cation Binding Ability', p. 97

R27 K. Naemura, Y. Tobe and T. Kaneda, 'Preparation of Chiral and Meso-crown Ethers Incorporating Cyclohexane-1,2-diol Derivatives as a Steric Barrier and their Complexation with Chiral and Achiral Amines', p. 199 1996, vol. 149

R28 J. Fraissard, R. Vincent, C. Doremieux, J. Karger and H. Pfeifer, 'Application of NMR Methods to Catalysis', p. 1

R29 D. J. Nelson, 'Aluminium Complexation with Nucleoside Di- and Triphosphates and Implication in Nucleoside Binding Proteins', p. 95

R30 J. M. Aramini, J. A. Saponja and H. J. Vogel, 'Spectroscopic Studies of the Interaction of Aluminum(III) with Transferrins', p. 193

1996, vol. 150

R31 I. Bertini and C. Luchinat, 'NMR of Paramagnetic Substances', p. 1 1996, vol. 151

R32 S. J. Berners-Price and P. J. Sadler, 'Coordination Chemistry of Metallodrugs: Insights into Biological Speciation from NMR Spectroscopy', p. 1 1996, vol. 154

R33 R. C. Fay, 'Stereochemistry and Molecular Rearrangements of Some Six-, Seven-, and Eight-Coordinate Chelates of Early Transition Metals', p. 99 1996, vol. 155

R34 P. S. Pregosin and R. Salzmann, 'Structure and Dynamics of Chiral Allyl Complexes of Pd(II): NMR Spectroscopy and Enantioselective Allylic Alkylation', p. 35

R35 E. Lindner, S. Pautz and M. Haustein, 'Dynamic, Reactivity and Catalytic Behavior of Pseudo-Undercoordinated Ruthenium and Rhodium Complexes Stabilized by Intramolecular Solvents', p. 145

Macromolecular Symposia, vol. 107, 1996

R36 S. Penczek and A. Duda, 'Selectivity as a Measure of "Livingness" of the Polymerization of Cyclic Esters', p. 1

NM R Basic Principles and Progress, ed. P. Diehl, E. Fluck, H. G�nther, R. Kosfeld and J. Seelig, Springer, Berlin, Germany, 1996, vol. 34

R37 N. Chandrakumar, 'Spin-1 NMR'

Progress in NM R Spectroscopy ed. J. W. Emsley, J. Feeney and L. H. Sutcliffe, 1996, vol. 28

R38 K. Asayama, Y. Kitaoka, G. Zheng and K. Ishida, 'NMR Studies of High Tc Superconductors', p. 221

R39 J. M. Miller, 'Fluorine-19 Magic-Angle Spinning NMR', p. 255

R40 J. A. Peters, J. Huskens and D. J. Raber, 'Lanthanide Induced Shifts and Relaxation Rate Enhancements', p. 283

1996, vol. 29

R41 J. C. Lindon, J. K. Nicholson and I. D. Wilson, 'Direct Coupling of Chromatographic Separations to NMR Spectroscopy', p. 1

R42 G. Varani, F. Aboul-ela and F. H. -T. Allain, 'NM R Investigation of RNA Structure', p. 51

R43 D. Farcasiu and A. Ghenciu, 'Determination of Acidity Functions and Acid Strengths by 13C NMR', p. 129

R44 F. Schick, 'Bone Marrow NMR In Vivo', p. 169

R45 A. C. de Dios, 'Ab Initio Calculations of the NMR Chemical Shift', p. 229

3 Edited Books and Symposia

ACS Symposia Series

R46 J. L. Bonardet, M. C. Barrage and J. Fraissard, 'NMR Techniques for Studying the Coking of Zeolite-Based Catalysts', 1996, 634, 99

R47 I. Ojima, S. D. Kuduk, J. C. Slater, R. H. Gimi, C. M. Sun, S. Chakravarty, M. Ourevitch, A. Abouabdellah, D. Bonnet-Delpon, et al., 'Syntheses, Biological Activity, and Conformational Analysis of Fluorine-Containing Taxoids', 1996, 639, 228

R48 J. M. Bortiatynski, P. G. Hatcher and H. Knicker, 'NMR Techniques (C, N, and H) in Studies of Humic Substances', 1996, 651, 57

R49 I. Bertini and C. Luchinat, 'Electronic Isomerism in Oxidized Fe4S4 High-Potential Iron-Sulfur Proteins', 1996, 653, 57

R50 G. Sakane and T. Shibahara, 'Characterization of Incomplete Cubane-Type and Cubane-Type Sulfur-Bridged Clusters', 1996, 653, 225

R51 R. C. Rayne and M. O'Shea, 'Neuropeptide Biosynthesis: Possible Molecular Targets for the Control of Insect Pests', 1997, 658, 292

Advances in Carbanion Chemistry

R52 S. Bradamante and G. A. Pagani, 'Benzyl and Heteroarylmethyl Carbanions: Structure and Substituent Effects', 1996, 2, 189

Bioactive Compound Design: Possibilities for Industrial Use, ed. M. G. Ford, R. Greenwood, G. T. Brooks and R. Franke, Bios Scientific Publishers, Oxford, UK, 1996

R53 H. Kubinyi, 'Computer-Aided Drug Design. Facts and Fictions', p. 1

Biochemical Aspects of Marine Pharmacology, ed. P. Lazarovici, M. Spira and E. Zlotkin, Alkan, Fort Collins, Colo., 1996

R54 Y. Kashman and A. Rudi, 'Bioactive Sponge and Ascidian Secondary Metabolites', p. 209

Bioenergetics: A Practical Approach, ed. G. C. Brown and C. E. Cooper, IRL Press, Oxford, UK, 1995

R55 K. M. Brindle, A. M. Fulton and S-P. Williams, 'Studies of Cellular Energetics Using 31P NMR', p. 159

Biological Membranes (A Molecular Perspective from Computation and Experiment), ed. K. M. Merz Jr. and B. Roux, Birkhauser, Boston, Mass., 1996

R56 M. F. Brown, 'Membrane Structure and Dynamics Studied with NMR Spectroscopy', p. 175

R57 R. R. Ketchem, B. Roux and T. A. Cross, 'Computational Refinement Through Solid State NMR and Energy Constraints of a Membrane Bound Polypeptide', p. 299

Biopolymer Mixtures, ed. S. E. Harding, S. E. Hill and J. R. Mitchell, Nottingham University Press, Nottingham, UK, 1995

R58 M. A. K. Williams, R. D. Keenan and T. K. Halstead, 'The Use of NMR in Characterizing Biopolymer Mixtures', p. 117

The Chemistry of Halides, Pseudo-Halides and Azides, ed. S. Patai and Z. Rappoport, Wiley, Chichester, UK, 1995 (Pt.1)

R59 P. Taylor and B. Everatt, 'NMR Spectroscopy', p. 267

R60 M. Geoffroy and E. A. C. Lucken, 'Electron Spin Resonance and Nuclear Quadrupole Resonance', p. 289

Complex Formation and Stereochemistry of Coordinating Compounds, ed. Y. Buslaev, Nova Science Publishers, Commack, N. Y., 1996

R61 G. Kirakosyan, 'NMR in the Study of Inorganic Complexes of the Noble Metals', p. 49

R62 V. I. Minkin and L. E. Nivorozhkin, 'Stereodynamics and Degenerated Ligand Exchange in the Solutions of Tetracoordinated Chelate Complexes of Non-Transition Metals', p. 77

Comprehensive Polymer Science, Second Supplement, ed. S. L. Aggarwal and S. Russo, Elsevier, Oxford, UK, 1996

R63 D. D. Werstler, 'Two-Dimensional NMR Spectroscopy for the Structural Characterization of Polymers', p. 197

Enzymology Labfax, ed. P. C. Engel, Academic, San Diego, Calif., 1996

R64 R. Cammack and J. K. Shergill, 'EPR Spectroscopy in Enzymology', p. 249

Evolutionary Biochemistry and Related Areas of Physicochemical Biology, ed. B. F. Poglazow, Bach Institute of Biochemistry, Moscow, Russia, 1995

R65 D. N. Ostrovsky, G. R. Diomina, E. I. Lysak and I. N. Shipanova, 'Novel Products and Participants of Oxidative Stress in Bacteria', p. 599

Free Radicals: A Practical Approach, ed. N. A. Punchard and F. J. Kelly, IRL Press, Oxford, UK, 1996

R66 D. P. Naughton, E. Lynch, G. E. Hawkes, J. Hawkes, D. R. Blake and M. Grootveld, 'Detection of Free Radicals Reaction Products by High-Field Magnetic Resonance Spectroscopy', p. 25

From Simplicity to Complexity in Chemistry – and Beyond, (Pt. 1), ed. A. Mueller, A. Dress and F. Voegtle, Vieweg & Sohn, Wiesbaden, Germany, 1996

R67 L. J. De Jongh, 'Physical Properties of High-Nuclearity Metal Cluster Compounds: Model Systems for Uniform-Sized Metal Particles', p. 163

Handbook of Metal-Ligand Interactions of Biological Fluids: Bioinorganic Medicine, ed. G. Berthon, Marcel Dekker, New York, 1995, vol. 1

R68 J. S. Valentine, 'Metal-Protein Interactions. Generalities on Metal Ion-Protein Interactions and their Investigation Techniques', p. 130

Handbook on the Physics and Chemistry of Rare Earths, ed. K. A. Gschneidner Jr. and L. Eyring, Elsevier, Amsterdam, Neth., 1996

R69 J. H. Forsberg, 'NMR Studies of Paramagnetic Lanthanide Complexes and Shift Reagents', p. 1

Handbook of Polymer-Fibre Composites., ed. F. R. Jones, Longman Scientific & Technical, Harlow, UK, 1994

R70 J. N. Hay, 'High Temperature Resins – Thermosetting Polyimides', p. 96

High Pressure Science and Technology, Proceedings of the Joint XV AIRAPT and XXXIII EHPRG International Conference, 1995, ed. W. A. Trzeciakowski, World Scientific, Singapore, 1996

R71 J. Jonas, 'NMR Studies of Pressure-Induced Reversible Unfolding of Proteins', p. 860

High Temperature Superconductivity: Models and Measurements, Proceedings of the 1994 GNSM School, ed. M. Acquarone, World Scientific, Singapore, 1996

R72 P. Carretta and A. Rigamonti, 'NMR-NQR Studies in Cuprates: from the Antiferromagnetic to the Superconducting State', p. 493.

Immobilised Living Cell Systems: Modelling and Experimental Methods, ed. R. G. Willaert, G. V. Baron and L. De Backer, Wiley, Chichester, UK, 1996

R73 E. J. Fernandez, 'Nuclear Magnetic Resonance Spectroscopy and Imaging', p. 117

Introduction to Biophysical Methods for Protein and Nucleic Acid Research., ed. J. A. Glasel and M. P. Deutscher, Academic, San Diego, 1995

R74 B. W. Bangerter, 'Nuclear Magnetic Resonance', p. 317

Ionomers Characterization, Theory, and Applications, ed. S. Schlick, CRC, Boca Raton, Fla., 1996

R75 S. Schlick and G. Gebel, 'NMR Spectroscopy of Bulk Perfluorinated Ionomers and Solutions: Information on Structure and Dynamics', p. 165

R76 G. Martini, S. Ristori and M. Visca, 'Self-Assembling of Perfluorinated Surfactants', p. 219

Lecture Notes of the Eighth Chinese International Summer School of Physics, Beijing, 1995, (Aspects of Modern Magnetism), ed. F. C. Pu, Y. J. Wang and C. H. Shang, World Scientific, Singapore, 1996

R77 Y. D. Zhang, J. I. Budnick and W. A. Hines, 'Applications of Nuclear Magnetic Resonance in the Study of Magnetic Materials', p. 236

Liquid Crystals in Complex Geometries Formed by Polymer and Porous Networks, ed. G. P. Crawford and S. Zumer, Taylor & Francis, London, UK, 1996

R78 M. Vilfan and N. Vrbancic-Kopac, 'Nuclear Magnetic Resonance of Liquid Crystals with an Embedded Polymer Network', p. 59

Moessbauer Spectroscopy Applied to Magnetism and Materials Science, vol. II, ed. G. J. Long and F. Grandjean, Plenum, New York, 1996

R79 C. Sauer, 'Magnetic and Structural Properties of Real Metal Layer Interfaces', p. 31

NATO Advanced Study Institute Series, Series A, 1996, vol. 288

R80 Y. Bai and S. W. Englander, 'The Cooperative Substructure of Protein Molecules', p. 1

R81 P. J. Connolly, A. S. Stem and J. C. Hoch, 'Solution Structure of the Long Neurotoxin LSIII with Possible Implications for Binding to the Acetylcholine Receptor', p. 29

R82 C. G. Hoogstraten and J. L. Markley, 'Approaches to the Determination of More Accurate Cross-Relaxation Rates and the Effects of Improved Distance Constraints on Protein Solution Structures', p. 73

R83 L. J. Smith and C. M. Dobson, 'Insights into Protein Dynamics by NMR Techniques', p. 127

R84 K. T. Dayie, G. Wagner and J. -F. Lefevre, 'Heteronuclear Relaxation and the Experimental Determination of the Spectral Density Function', p. 139

R85 A. Ramamoorthy, F. M. Marassi and S. J. Opella, 'Applications of Multidimensional Solid-State NMR Spectroscopy to Membrane Proteins', p. 237

Series C, 1996, vol. 480

R86 J. A. Ripmeester and C. I. Ratcliffe, 'Solid-State NMR in Inclusion Compounds. Synoptic Approaches to Structure Determination', p. 101

1996, vol. 485

R87 H.-J. Schneider and J. Sartorius, 'An Incremental Empirical Approach to Noncovalent Interactions in and with DNA', p. 11

R88 J. L. Dye, 'Magnetic, Electrical and Spectroscopic Studies of Alkalides and Electrides. Experimental Methods and Examples', p. 313

R89 Z. Chen, L. Mercier, J. J. Tunney and C. Detellier, 'Dynamics of Supramolecular Assemblies in Solution and Solid State', p. 393

Series E, 1996, vol. 320

R90 S. Hanessian, 'Target-Driven Organic Synthesis: Reflections on the Past, Prospects for the Future', p. 61

1996, Vol. 327

R91 Y. Morishima, 'Unimolecular Micelles of Hydrophobically Modified Polyelectrolytes', p. 331

NMR Spectroscopy Techniques: Second Edition, Revised and Expanded. [In: Practical Spectroscopy, 1996;21], ed. M. D. Bruch, Marcel Dekker, New York, 1996, 616 pp

R92 D. D. Traficante, 'NMR Concepts', p. 1

R93 M. D. Bruch and C. Dybowski, 'Spectral Editing Methods for Structure Elucidation', p. 61

R94 R. E. Wasylishen, 'NMR Relaxation and Dynamics', p. 105

R95 M. D. Bruch, 'Multidimensional NMR Spectroscopy of Liquids', p. 145

R96 C. K. McClure, 'Small Organic Molecules: Practical Tips and Structure Elucidation', p. 239

R97 J. Rizo and M. D. Bruch, 'Structure Determination of Biological Macromolecules', p. 285

(Continues...)

Excerpted from Nuclear Magnetic Resonance Volume 27 by G. A. Webb. Copyright � 1998 The Royal Society of Chemistry. Excerpted by permission of The Royal Society of Chemistry.
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