Moderne Methoden der Pflanzenanalyse / Modern Methods of Plant Analysis

Language: English

Published by Springer Vieweg, 2011

3642649602 / 9783642649608

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Seller: AHA-BUCH GmbH, Einbeck, GermanyAHA-BUCH GmbH

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Druck auf Anfrage Neuware - Printed after ordering - If, following the solvent extraction of a hydrocarbon from a plant, it is not known whether it is one or the other, a method of distinguishing the two is described by HENDRICKS, WILDMAN and JONES (1946). The technique involves the infra-red absorption spectra of the two isomers. At about 12 mp. the relative absorption coefficient of rubber is 42% greater than for gutta. ScHLESINGER and LEPER (1951) describe two procedures for separation of the rubber and gutta hydrocarbons from large quantities of crude chicle. In one, the chicle is extracted with benzene which dissolves both isomers. An excess absolute ethyl acetate is added and the mixture stored at 5° C overnight. The gutta precipitates out and the rubber remains in solution. The other method is as follows: (1) Ten grams of chicle are extracted with acetone for 24 hours in a Soxhlet extraction apparatus. (2) The insoluble material in the thimble is allowed to . it dry, then immersed in 150 ml. of cold Skellysolve B in a refrigerator at 10° C and allowed to stand for 48 hours with occasional agitation. (3) The thimble is then removed from the solvent and the enclosed residue washed several times with fresh, cold Skellysolve B. (4) An excess of acetone and a few drops of a concentrated aqueous solution of sodium iodide are added to the combined Skellysolve B extract and washings and allowed to stand overnight in a refrigerator.

Seller Inventory # 9783642649608

Title
Moderne Methoden der Pflanzenanalyse / Modern Methods of Plant Analysis
Author
K. Paech
Publisher
Springer Vieweg
Publication year
2011
Condition
Neu
Binding
Taschenbuch
Language
English
ISBN 10
3642649602
ISBN 13
9783642649608
Item weight
1,205 grams
Dimensions
244x156x42 mm

AHA-BUCH GmbH

Einbeck, Germany

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