Analytical Method Development and Validation: Simultaneous Estimation of Pioglitazone and Glimepiride in Tablet Dosage Form by RP-HPLC - Softcover
Synopsis
A simple reverse phase liquid Chromatographic method has been developed and subsequently validated for simultaneous determination of Pioglitazone and Glimepiride in combination. The separation was carried out using a mobile phase of phosphate buffer (pH-4.5): Acetonitrile (45:55) v/v and using methanol as diluent. The column used was Inertsil ODS (250 mm x 4.6 mm i.d., 5μm) with flow rate of 1 ml/min using UV detection at 225 nm. The described method was linear over a concentration range of 5-50μg/ml and 5-25 μg/ml for the assay of Pioglitazone and Glimepiride respectively. The retention times of Pioglitazone and Glimepiride were found to be4.6 and 7.7min respectively. Results of analysis were validated statistically and by recovery studies. The results of the study showed that the proposed RP-HPLC method is simple, rapid, precise and accurate, which is useful for the routine determination of Pioglitazone and Glimepiride bulk drug and in its pharmaceutical dosage form.
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About the Author
Gagan Sharma is a young dynamic amateur researcher, born on 19 Nov. 1985. Gagan has earned Master of Pharmacy (Pharmaceutical chemistry) from NMIMS University Mumbai (India). Gagan has extensive exposer in pharmaceutical Technology Transfer and Quality Assurance.
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Analytical Method Development and Validation
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LAP LAMBERT Academic Publishing Sep 2012, 2012
ISBN 10: 3659253995
ISBN 13: 9783659253997
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Taschenbuch. Condition: Neu. This item is printed on demand - it takes 3-4 days longer - Neuware -A simple reverse phase liquid Chromatographic method has been developed and subsequently validated for simultaneous determination of Pioglitazone and Glimepiride in combination. The separation was carried out using a mobile phase of phosphate buffer (pH-4.5): Acetonitrile (45:55) v/v and using methanol as diluent. The column used was Inertsil ODS (250 mm x 4.6 mm i.d., 5 m) with flow rate of 1 ml/min using UV detection at 225 nm. The described method was linear over a concentration range of 5-50 g/ml and 5-25 g/ml for the assay of Pioglitazone and Glimepiride respectively. The retention times of Pioglitazone and Glimepiride were found to be4.6 and 7.7min respectively. Results of analysis were validated statistically and by recovery studies. The results of the study showed that the proposed RP-HPLC method is simple, rapid, precise and accurate, which is useful for the routine determination of Pioglitazone and Glimepiride bulk drug and in its pharmaceutical dosage form. 112 pp. Englisch. Seller Inventory # 9783659253997
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Analytical Method Development and Validation
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ISBN 13: 9783659253997
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Condition: New. Dieser Artikel ist ein Print on Demand Artikel und wird nach Ihrer Bestellung fuer Sie gedruckt. Autor/Autorin: Sharma GaganGagan Sharma is a young dynamic amateur researcher, born on 19 Nov. 1985. Gagan has earned Master of Pharmacy (Pharmaceutical chemistry) from NMIMS University Mumbai (India). Gagan has extensive exposer in pharmaceutical. Seller Inventory # 5143338
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Analytical Method Development and Validation
Published by
LAP LAMBERT Academic Publishing Sep 2012, 2012
ISBN 10: 3659253995
ISBN 13: 9783659253997
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Taschenbuch. Condition: Neu. This item is printed on demand - Print on Demand Titel. Neuware -A simple reverse phase liquid Chromatographic method has been developed and subsequently validated for simultaneous determination of Pioglitazone and Glimepiride in combination. The separation was carried out using a mobile phase of phosphate buffer (pH-4.5): Acetonitrile (45:55) v/v and using methanol as diluent. The column used was Inertsil ODS (250 mm x 4.6 mm i.d., 5¿m) with flow rate of 1 ml/min using UV detection at 225 nm. The described method was linear over a concentration range of 5-50¿g/ml and 5-25 ¿g/ml for the assay of Pioglitazone and Glimepiride respectively. The retention times of Pioglitazone and Glimepiride were found to be4.6 and 7.7min respectively. Results of analysis were validated statistically and by recovery studies. The results of the study showed that the proposed RP-HPLC method is simple, rapid, precise and accurate, which is useful for the routine determination of Pioglitazone and Glimepiride bulk drug and in its pharmaceutical dosage form.VDM Verlag, Dudweiler Landstraße 99, 66123 Saarbrücken 112 pp. Englisch. Seller Inventory # 9783659253997
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Analytical Method Development and Validation : Simultaneous Estimation of Pioglitazone and Glimepiride in Tablet Dosage Form by RP-HPLC
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LAP LAMBERT Academic Publishing, 2012
ISBN 10: 3659253995
ISBN 13: 9783659253997
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Taschenbuch. Condition: Neu. nach der Bestellung gedruckt Neuware - Printed after ordering - A simple reverse phase liquid Chromatographic method has been developed and subsequently validated for simultaneous determination of Pioglitazone and Glimepiride in combination. The separation was carried out using a mobile phase of phosphate buffer (pH-4.5): Acetonitrile (45:55) v/v and using methanol as diluent. The column used was Inertsil ODS (250 mm x 4.6 mm i.d., 5 m) with flow rate of 1 ml/min using UV detection at 225 nm. The described method was linear over a concentration range of 5-50 g/ml and 5-25 g/ml for the assay of Pioglitazone and Glimepiride respectively. The retention times of Pioglitazone and Glimepiride were found to be4.6 and 7.7min respectively. Results of analysis were validated statistically and by recovery studies. The results of the study showed that the proposed RP-HPLC method is simple, rapid, precise and accurate, which is useful for the routine determination of Pioglitazone and Glimepiride bulk drug and in its pharmaceutical dosage form. Seller Inventory # 9783659253997
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Analytical Method Development and Validation | Simultaneous Estimation of Pioglitazone and Glimepiride in Tablet Dosage Form by RP-HPLC
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ISBN 10: 3659253995
ISBN 13: 9783659253997
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Taschenbuch. Condition: Neu. Analytical Method Development and Validation | Simultaneous Estimation of Pioglitazone and Glimepiride in Tablet Dosage Form by RP-HPLC | Gagan Sharma (u. a.) | Taschenbuch | 112 S. | Englisch | 2012 | LAP LAMBERT Academic Publishing | EAN 9783659253997 | Verantwortliche Person für die EU: preigu GmbH & Co. KG, Lengericher Landstr. 19, 49078 Osnabrück, mail[at]preigu[dot]de | Anbieter: preigu. Seller Inventory # 106239465
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Analytical Method Development and Validation: Simultaneous Estimation of Pioglitazone and Glimepiride in Tablet Dosage Form by RP-HPLC
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LAP LAMBERT Academic Publishing, 2012
ISBN 10: 3659253995
ISBN 13: 9783659253997
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