Modification of an Nbs Reference Spectrophotometer (Classic Reprint) - Softcover

Eckerle, Kenneth L.

 
9781390476293: Modification of an Nbs Reference Spectrophotometer (Classic Reprint)

Synopsis

Excerpt from Modification of an Nbs Reference Spectrophotometer

A pneumatically controlled sliding sample holder was constructed. The temperature of samples mounted in this holder is controlled by water circulated in the holder and in a jacket surrounding the filter to also maintain the temperature of the air surrounding the filter. The holder - jacket combination is three point spring loaded.

The circulating water temperature is provided by a bath which was modified. The heaters and refrigerator (approximately 670 watts each) of the bath were isolated and ad justed so that in combination they yield a nearly constant temperature. Then, a 300 watt heater was installed to tune the temperature to the desired level. A special proportional controller was obtained which shuts off the heater or refrigerator (depending on whether one desires a lower or higher temperature) for large temperature changes (several degrees C) until the temperature reaches the range where the 300 watt heater is cycled to maintain a constant temperature as detected by a thermistor placed in the bath.

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