Handbook of High Field Dynamic Nuclear Polarization (eMagRes Books) - Hardcover

Hardcover

ISBN 10: 1119441641 ISBN 13: 9781119441649

Publisher: Wiley, 2020

Synopsis

Addresses Dynamic Nuclear Polarization (DNP) as a technique for sensitivity-enhancement in solid-state NMR spectroscopy

This comprehensive handbook is a compendium of the current state-of-the art of high field Dynamic Nuclear Polarization―from long-proven, early developments, up to today’s hot topics. It covers all the relevant subjects that have made a direct or indirect contribution toward advancing this field, and focuses on topics such as: the theory behind the effects seen within DNP; instrumentation required for carrying out DNP; and specific applications of DNP including protein monitoring, catalysis, nanoparticles, biological and clinical studies. Development and application of techniques that have indirectly contributed to advancing MAS DNP NMR, such as DNP experiments on static solids within microwave resonant structures, and high-field EPR, are also examined.

Handbook of High Field Dynamic Nuclear Polarization is presented in three sections―Theoretical Aspects, DNP Development (instrumentation / radical / sample), and DNP NMR Applications. The first section offers chapters on; solid and cross effect DNP; thermal mixing; Overhauser; and dissolution DNP. The second looks at: microwave technology, gyrotron, and IOE; homebuilt and commercial DNP spectrometers; and glassing vs. solvent-free DNP. The final section provides information on; amyloid, membrane, and nanocrystalline proteins; metals, and surface enhanced DNP; pharmaceuticals; nanoparticles; and much more. 

• Covers one of the biggest developing fields in magnetic resonance
• Relevant to students, academics, and industry within the physical, materials, medical, and biochemical sciences
• An excellent starting point and point-of-reference for researchers in the field
• Edited by a widely respected team with contributions from key researchers in the NMR community
• Part of the eMagRes Handbook Series

Handbook of High Field Dynamic Nuclear Polarization is an ideal reference for all researchers and graduate students involved in this complex, interdisciplinary field.

About eMagRes Handbooks

eMagRes publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of eMagRes articles. In consultation with the eMagRes Editorial Board, the eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.

Have the content of this Handbook and the complete content of eMagRes at your fingertips!

Visit: www.wileyonlinelibrary.com/ref/eMagRes

About this title

About the Author

Editors

Vladimir K. Michaelis is Assistant Professor in the Department of Chemistry at the University of Alberta.

Robert G. Griffin is Professor of Chemistry and Director of the Francis Bitter Magnet Laboratory at the Massachusetts Institute of Technology.

Björn Corzilius is Professor of Physical Chemistry in the Institute of Chemistry at the University of Rostock.

Shimon Vega is Professor in the Department of Chemical Physics at the Weizmann Institute of Science, Israel.

From the Back Cover

HANDBOOK OF HIGH FIELD DYNAMIC NUCLEAR POLARIZATION

Addresses Dynamic Nuclear Polarization (DNP) as a technique for sensitivity-enhancement in solid-state NMR spectroscopy

This comprehensive handbook is a compendium of the current state-of-the art of high field Dynamic Nuclear Polarization from long-proven, early developments, up to today's hot topics. It covers all the relevant subjects that have made a direct or indirect contribution toward advancing this field, and focuses on topics such as: the theory behind the effects seen within DNP; instrumentation required for carrying out DNP; and specific applications of DNP including protein monitoring, catalysis, nanoparticles, biological and clinical studies. Development and application of techniques that have indirectly contributed to advancing MAS DNP NMR, such as DNP experiments on static solids within microwave resonant structures, and high-field EPR, are also examined.

Handbook of High Field Dynamic Nuclear Polarization is presented in two sections Concepts, Theory, & Instrumentation and Applications. The first section includes chapters on: solid and cross effect DNP; thermal mixing; Overhauser; cryogenic platforms; dissolution DNP; homebuilt and commercial DNP spectrometers. The second section provides information on: amyloid, membrane, and nanocrystalline proteins; metals and surface enhanced DNP; pharmaceuticals; nanoparticles; and much more.

• Covers one of the biggest developing fields in magnetic resonance
• Relevant to students, academics, and industry within the physical, materials, medical, and biochemical sciences
• An excellent starting point and point-of-reference for researchers in the field
• Edited by a widely respected team with contributions from key researchers in the NMR community
• Part of the eMagRes Handbook Series

Handbook of High Field Dynamic Nuclear Polarization is an ideal reference for all researchers and graduate students involved in this complex, interdisciplinary field.

About eMagRes Handbooks

eMagRes publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of eMagRes articles. In consultation with the eMagRes Editorial Board, the eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.

Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes

From the Inside Flap

HANDBOOK OF HIGH FIELD DYNAMIC NUCLEAR POLARIZATION

Addresses Dynamic Nuclear Polarization (DNP) as a technique for sensitivity-enhancement in solid-state NMR spectroscopy

This comprehensive handbook is a compendium of the current state-of-the art of high field Dynamic Nuclear Polarization—from long-proven, early developments, up to today's hot topics. It covers all the relevant subjects that have made a direct or indirect contribution toward advancing this field, and focuses on topics such as: the theory behind the effects seen within DNP; instrumentation required for carrying out DNP; and specific applications of DNP including protein monitoring, catalysis, nanoparticles, biological and clinical studies. Development and application of techniques that have indirectly contributed to advancing MAS DNP NMR, such as DNP experiments on static solids within microwave resonant structures, and high-field EPR, are also examined.

Handbook of High Field Dynamic Nuclear Polarization is presented in two sections — Concepts, Theory, & Instrumentation and Applications. The first section includes chapters on: solid and cross effect DNP; thermal mixing; Overhauser; cryogenic platforms; dissolution DNP; homebuilt and commercial DNP spectrometers. The second section provides information on: amyloid, membrane, and nanocrystalline proteins; metals and surface enhanced DNP; pharmaceuticals; nanoparticles; and much more.

• Covers one of the biggest developing fields in magnetic resonance
• Relevant to students, academics, and industry within the physical, materials, medical, and biochemical sciences
• An excellent starting point and point-of-reference for researchers in the field
• Edited by a widely respected team with contributions from key researchers in the NMR community
• Part of the eMagRes Handbook Series

Handbook of High Field Dynamic Nuclear Polarization is an ideal reference for all researchers and graduate students involved in this complex, interdisciplinary field.

About eMagRes Handbooks

eMagRes publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of eMagRes articles. In consultation with the eMagRes Editorial Board, the eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.

Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes

Edition details

• Publisher: Wiley
• Publication date: 2020
• Language: English
• ISBN 10: 1119441641
• ISBN 13: 9781119441649
• Binding: Hardcover
• Edition number: 1
• Number of pages: 472
• Editor: Michaelis Vladimir K., Griffin Robert G., Corzilius Björn, Vega Shimon