Written for a course that deals with the principles and applications of modern analytical instruments, this edition reflects updated techniques and a more applied approach with the addition of case studies. Emphasis is placed upon the theoretical basis of each type of instrument, its optimal area of application, its sensitivity, its precision, and its limitations. The text also introduces students to elementary integrated circuitry, microprocessors and computers, and treatment of analytical data. A text-specific CD-ROM accompanies all new copies of the text, providing students with excel files of data analysis and simulations of analytical techniques to help them visualize important concepts in this course. Written for a course that deals with the principles and applications of modern analytical instruments, this edition reflects updated techniques and a more applied approach with the addition of case studies. Emphasis is placed upon the theoretical basis of each type of instrument, its optimal area of application, its sensitivity, its precision, and its limitations. The text also introduces students to elementary integrated circuitry, microprocessors and computers, and treatment of analytical data. A text-specific CD-ROM accompanies all new copies of the text, providing students with excel files of data analysis and simulations of analytical techniques to help them visualize important concepts in this course.
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1. Introduction. Section I. MEASUREMENT BASICS. 2. Electrical Components and Circuits. 3. Operational Amplifiers in Chemical Instrumentation. 4. Digital Electronics and Microcomputers. 5. Signals and Noise. Instrumental Methods in Action: Assessing the Authenticity of the Vinland Map. Section II. ATOMIC SPECTROSCOPY. 6. An Introduction to Spectrometric Methods. 7. Components of Optical Instruments. 8. An Introduction to Optical Atomic Spectrometry. 9. Atomic Absorption and Atomic Fluorescence Spectrometry. 10. Atomic Emission Spectrometry. 11. Atomic Mass Spectrometry. 12. Atomic X-Ray Spectrometry. Instrumental Methods in Action: Title. Section III. MOLECULAR SPECTROSCOPY. 13. An Introduction to Ultraviolet/Visible Molecular Absorption Spectrometry. 14. Applications of Ultraviolet/Visible Molecular Absorption Spectrometry. 15. Molecular Luminescence Spectrometry. 16. An Introduction to Infrared Spectrometry. 17. Applications of Infrared Spectrometry. 18. Raman Spectroscopy. 19. Nuclear Magnetic Resonance Spectroscopy. 20. Molecular Mass Spectrometry. 21. Surface Characterization by Spectroscopy and Microscopy. Instrumental Methods in Action: Title. Section IV. ELECTROANALYTICAL CHEMISTRY. 22. Introduction to Electroanalytical Chemistry. 23. Potentiometry. 24. Coulometry. 25. Voltammetry. Instrumental Methods in Action: Title. Section V. SEPARATION METHODS. 26. An Introduction to Chromatographic Separations. 27. Gas Chromatography. 28. High-Performance Liquid Chromatography. 29. Supercritical Fluid Chromatography and Extraction. 30. Capillary Electrophoresis and Capillary Electrochromatography. Instrumental Methods in Action: Title. Section VI. MISCELLANEOUS METHODS. 31. Thermal Methods. 32. Radiochemical Methods. 33. Automated Methods of Analysis. 34. Particle Size Analysis. Instrumental Methods in Action: Title. Appendices. Appendix 1. Evaluation of Analytical Data. Appendix 2. Some Standard and Formal Electrode Potentials. Appendix 3. Compounds for Preparing Standard Solutions of Some Common Elements. Appendix 4. Common Acronyms Encountered in Chemical Instrumentation. Answers to Selected Problems. Index.
Douglas A. Skoog was a professor of chemistry at Stanford University and the lead author of several best-selling texts during his career. He earned a B.S. in chemistry from Oregon State University and his Ph.D. in analytical chemistry from the University of Illinois. Dr. Skoog was the 1999 recipient of the American Chemical Society award in analytical chemistry, sponsored by the Fisher Scientific Company. That same year, he was named a fellow of the American Association for the Advancement of Science. In 1993, he received the ACS Division of Analytical Chemistry Award for Excellence in Teaching. F. James Holler is professor emeritus of chemistry and recipient of the Alumni Association Great Teacher Award at the University of Kentucky. He received his Ph.D. from Michigan State University. In addition to his role as co-author of several bestselling texts, he is co-creator of the world-famous Periodic Table of Comic Books. Stanley R. Crouch is professor emeritus at Michigan State University. He received his undergraduate and M.S. degrees from Stanford University and his Ph.D. in analytical chemistry from the University of Illinois. He is the recipient of the 2001 American Chemical Society Division of Analytical Chemistry Award in Chemical Instrumentation and the 1996 ACS Division of Analytical Chemistry Award for Excellence in Teaching.
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