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Synopsis
Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
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George H. Stout and Lyle H. Jensen are the authors of X-Ray Structure Determination: A Practical Guide, 2nd Edition, published by Wiley.
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X-Ray Structure Determination: A Practical Guide, 2nd Edition
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X-Ray Structure Determination : A Practical Guide
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Wiley & Sons, Incorporated, John, 1989
ISBN 10: 0471607118
ISBN 13: 9780471607113
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