Introduction to Semimicro Qualitative Analysis

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9780130462169: Introduction to Semimicro Qualitative Analysis

For courses in General Chemistry (Lecture and Laboratory) and Qualitative Inorganic Analysis.

 

This self-teaching lab manual presents a process for learning descriptive chemistry and the chemistry of the more common elements and their compounds in the format of a scheme of analysis. Students and challenged to call upon their manipulative and observational skills to provide the basis for identifying a substance or a mixture of substances. Part I describes the strategy of qualitative analysis so that students have a review of the principles readily available when they are engaged in the details of laboratory work; Part II presents the concepts involved in qualitative analysis, systematically dealing with the nature of the chemical compounds; Part III features well-tested analytical laboratory procedures.

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Semimicro Qualitative Analysis, Eighth Edition, addresses two important current issues in chemistry education: the need for students to acquire a knowledge of descriptive chemistry and a growing interest by teaching chemists to expose students to the concepts of "green chemistry."

Although descriptive chemistry may be difficult to define precisely, most chemists would agree that a major component of this subject—descriptive chemistry—is the chemistry of the more common elements and their compounds, especially as this occurs in aqueous solutions.

"Green chemistry," briefly, is an expression of doing chemistry—laboratory work—that minimizes the use of chemicals, uses benign solvents (like water); and attends to the problems of handling "wastes" in a non-polluting way.

The first part of this classic work discusses the general strategy of qualitative analysis. It then systematically surveys the nature of chemical compounds including ionic, covalent and coordination of compounds, and the chemical reactions they undergo.

The second part provides a series of laboratory experiments to perform that have been tested over time, and reviewed to insure current treatment in terms of chemical safety and disposal. Key chemical concepts are highlighted along with important safety information. The discussion in Part I provides a firm foundation for understanding the practical work carried out in Part II.

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Book Description Prentice Hall, 2004. Book Condition: New. Brand New, Unread Copy in Perfect Condition. A+ Customer Service! Summary: CONTENTS Part I GENERAL STRATEGY 1 The Strategy of Qualitative Analysis Summary Part II CONCEPTS IN QUALITATIVE ANALYSIS 2 The Nature of Chemical Reactions Kinetics Chemical Equilibrium Thermodynamics Summary 3 The Nature of Chemical Compounds Physical Properties of Compounds Classification of Chemical compounds The Ionization of Water Acids and Bases 4 Solution Phenomena Concentration Units Solubility Equilibrium Processes Involving Sparingly Soluble Ionic Substances Colloidal dispersions 5 Complex Compounds Lewis Theory of Chemical Combinations Nomenclature Theoretical Considerations Stability of Complex Ions The Role of Complex Ions in Qualitative Analysis 6 Oxidation Reduction Reactions Part III THE PRACTICE OF QUALITATIVE ANALYSIS 7 The Practical Aspects of Qualitative Analysis The Periodic Table Chemical Reactions Equilibrium Considerations Formation of Precipitates Dissolving Precipitates Laboratory Safety 8 Laboratory Practices Summary of Laboratory Work Record of Laboratory Work and Laboratory Reports Laboratory Procedures 9 The Silver Group The Chemistry of the Silver Group Ions Precipitation and Analysis of the Silver Group Separation of Lead from Silver and Mercury (I) Separation and Detection of Silver and Mercury 10 The Copper-Arsenic Group The Chemistry of the Copper-Arsenic Group Ions Separation of the Copper Subgroup from the Arsenic Subgroup Separation of Mercury from Lead, Bismuth, Copper, and Cadmium Separation of Lead from Bismuth, Copper, and Cadmium Separation of Bismuth from Copper and Cadmium Detection of Copper and Cadmium Separation of Arsenic from Antimony and Tin 11 The Aluminum-Nickel Group The chemistry of the Aluminum-Nickel Group Ions Precipitation and Analysis of the Aluminum-Nickel Group Separation of the Aluminum Subgroup from the Nickel Subgroup Detection of Iron, Cobalt, Nickel, and Manganese 12 The Barium-Magnesium Group The Chemistry of the Barium-Magnesium Group Ions Detection of Ammonium Salts The Separation and Detection of Barium The Separation and Detection of Calcium Detection of Sodium and Potassium 13 The Analysis of Alloys 14 Analysis of Salts and Salt Mixtures Examination of the Solid Solubility of the Salt Reactions with Specific Reagents Preliminary Experiments Analysis of Unknown Salt Examination of the Solid Dissolution of the Solid Determine What Cations Are Present Treatment of the Unknown with Class Reagents Specific Tests for Anions 15 Recording and Reporting Analysis APPENDICES I Brief Review of Oxidation Numbers II Solution of Quadratic Equations III Reagents and Equipment Used Index of Procedures Index. Bookseller Inventory # ABE_book_new_0130462160

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